HBr*L-Ala-ψ-L-Ala-OBzl

Base Information

Chemical Name:HBr*L-Ala-ψ-L-Ala-OBzl
CAS No.:137234-24-3
Molecular Formula:BrH*C₁₃H₁₇N₅O₂
Molecular Weight:356.222
Hs Code.:

Synonyms:HBr*L-Ala-ψ-L-Ala-OBzl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of HBr*L-Ala-ψ-L-Ala-OBzl

Chemical Property:

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Technology Process of HBr*L-Ala-ψ-L-Ala-OBzl

There total 1 articles about HBr*L-Ala-ψ-L-Ala-OBzl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.3%

: 133641-24-4
Z-L-Ala-ψ-L-Ala-OBzl

: 137234-24-3
HBr*L-Ala-ψ-L-Ala-OBzl

Guidance literature:: With hydrogen bromide; In acetic acid; for 0.333333h; Ambient temperature;
DOI:10.1021/jo00027a038

Reference yield: 66.6%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 137234-24-3
HBr*L-Ala-ψ-L-Ala-OBzl

: 137234-21-0
Boc-Phe-Ala-ψ-Ala-OBzl

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; N,N-dimethyl-formamide; a) -10 deg C, 1 h, b) r.t., overnight;
DOI:10.1021/jo00027a038

Reference yield:

: 137234-24-3
HBr*L-Ala-ψ-L-Ala-OBzl

: 137259-48-4
Boc-Phe-Ala-ψ-Ala-OH

Guidance literature:: Multi-step reaction with 2 steps

1: 66.6 percent / isobutylchloroformate, N-methylmorpholine / CH₂Cl₂; dimethylformamide / a) -10 deg C, 1 h, b) r.t., overnight

2: 84.9 percent / acetic acid, H₂ / 10percent Pd/C / ethanol

With 4-methyl-morpholine; hydrogen; acetic acid; isobutyl chloroformate; palladium on activated charcoal; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00027a038