(8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

Base Information

Chemical Name:(8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid
CAS No.:302945-23-9
Molecular Formula:C₁₈H₁₃NO₈
Molecular Weight:371.303
Hs Code.:

(8-methoxycarbonyloxy-2,4-dioxo-4<i>H</i>-benzo[<i>e</i>][1,3]oxazin-3-yl)-phenyl-acetic acid

Synonyms:(8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

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Chemical Property of (8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

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Technology Process of (8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

There total 3 articles about (8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 875-74-1
(R)-phenylglycine

: 201296-89-1
(2,3-dimethoxycarbonyloxy)benzoyl chloride

: 302945-23-9
(8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

Guidance literature:: With sodium hydrogencarbonate; In tetrahydrofuran; at 0 - 3 ℃; for 1h;

Reference yield:

: 303-38-8
2,3-Dihydroxybenzoic acid

: 302945-23-9
(8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 61 percent / aq. NaOH / H₂O / 0.17 h / 0 - 3 °C

2: 1.99 g / PCl₅ / CCl₄ / 50 °C

3: 49 percent / aq. NaHCO₃ / tetrahydrofuran / 1 h / 0 - 3 °C

With sodium hydroxide; phosphorus pentachloride; sodium hydrogencarbonate; In tetrahydrofuran; tetrachloromethane; water; 1: Acylation / 2: Chlorination / 3: Condensation;

Reference yield:

: 222320-82-3
(2,3-dimethoxycarbonyloxy)benzoic acid

: 302945-23-9
(8-methoxycarbonyloxy-2,4-dioxo-4H-benzo[e][1,3]oxazin-3-yl)-phenyl-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.99 g / PCl₅ / CCl₄ / 50 °C

2: 49 percent / aq. NaHCO₃ / tetrahydrofuran / 1 h / 0 - 3 °C

With phosphorus pentachloride; sodium hydrogencarbonate; In tetrahydrofuran; tetrachloromethane; 1: Chlorination / 2: Condensation;