((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

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Chemical Name:((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone
CAS No.:928118-89-2
Molecular Formula:C₁₉H₂₉NO₃
Molecular Weight:319.444
Hs Code.:

Synonyms:((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

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Chemical Property of ((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

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Technology Process of ((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

There total 1 articles about ((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 4784-77-4,39616-19-8,29576-14-5
(E)-1-Bromo-2-butene

: 115512-81-7
(S)-2-methoxy-1-[[2'-(methoxymethyl)pyrrolidinyl]carbonyl]-5-methylbenzene

: 928118-89-2
((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

: ((S)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

Guidance literature:: (S)-2-methoxy-1-[[2'-(methoxymethyl)pyrrolidinyl]carbonyl]-5-methylbenzene; With ammonia; lithium; In tetrahydrofuran; tert-butyl alcohol; at -78 ℃; for 0.333333h;

(E)-1-Bromo-2-butene; In tetrahydrofuran; tert-butyl alcohol; at -78 - 20 ℃;
DOI:10.1021/jo0621423

Reference yield: 99.0%

: 928118-89-2
((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

: 928119-06-6
((R)-2-((E)-but-2-enyl)-2-((S)-2-methoxymethyl)pyrrolidine-1-carbonyl)-4-methylcyclohex-3-enone

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃; for 15h;
DOI:10.1021/jo0621423

Reference yield:

: 928118-89-2
((R)-1-((E)-but-2-enyl)-2-methoxy-5-methylcyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)-pyrrolidin-1-yl)methanone

: (R)-4-((S)-but-3-en-2-yl)-2-((S)-2-(methoxymethyl)pyrrolidine-1-carbonyl)-4-methylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / HCl / methanol / 15 h / 20 °C

2: 70 percent / 1,2-dichloro-benzene / 10 h / Heating

With hydrogenchloride; In methanol; 1,2-dichloro-benzene; 2: Cope rearrangement;
DOI:10.1021/jo0621423