(3S,6S)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

Base Information

Chemical Name:(3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid
CAS No.:102115-96-8
Molecular Formula:C₂₀H₂₆N₂O₉
Molecular Weight:438.434
Hs Code.:

Synonyms:(3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

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Chemical Property of (3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

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Technology Process of (3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

There total 1 articles about (3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 102115-95-7
3-benzyloxycarbonyl-1-<<(tert-butoxycarbonyl)amino>methyl>-2-oxa-3-azabicyclo<2.2.2>oct-5-ene

: 102115-96-8
(3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

Guidance literature:: With potassium permanganate; tetra(n-butyl)ammonium hydrogensulfate; In water; benzene; at 25 ℃;
DOI:10.1039/c39850001549

Reference yield: 4.8%

: 501-53-1,94274-21-2
benzyl chloroformate

: 102115-96-8
(3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

: 102115-97-9
(3S*,6S*)-2,3-bis(benzyloxycarbonyl)-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-6-carboxylic acid

: 108634-95-3
dibenzyl (3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylate

Guidance literature:: With pyridine; In dichloromethane; Ambient temperature;
DOI:10.1016/S0040-4020(01)87377-4

Reference yield:

: 102115-96-8
(3S*,6S*)-2-benzyloxycarbonyl-6-<<(tert-butoxycarbonyl)amino>methyl>perhydro-1,2-oxazine-3,6-dicarboxylic acid

: 65709-93-5,102209-37-0,137764-24-0
(+/-)-tabtoxinine-β-lactam

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / pyridine / CH₂Cl₂ / 25 °C

2: 99 percent / 98percent formic acid / 3 h / 25 °C

3: 63 percent / Ph₃P, di-2-pyridyl disulphide / acetonitrile / 2 h / 80 °C

4: 100 percent / H₂ / 10percent Pd/C / ethanol

With pyridine; formic acid; 2,2'-dipyridyldisulphide; hydrogen; triphenylphosphine; palladium on activated charcoal; In ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c39850001549