C₄₅H₅₀O₁₃

Base Information

Chemical Name:C₄₅H₅₀O₁₃
CAS No.:949159-01-7
Molecular Formula:C₄₅H₅₀O₁₃
Molecular Weight:798.884
Hs Code.:

C<sub>45</sub>H<sub>50</sub>O<sub>13</sub>

Synonyms:C₄₅H₅₀O₁₃

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Chemical Property of C₄₅H₅₀O₁₃

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Technology Process of C₄₅H₅₀O₁₃

There total 14 articles about C₄₅H₅₀O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 949159-00-6
C₅₄H₇₀O₁₃Si

: 949159-01-7
C₄₅H₅₀O₁₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ol0713335

Reference yield:

: 1-O-allyl-3-O-methyl-4,6-benzylidene-D-mannose

: 949159-01-7
C₄₅H₅₀O₁₃

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / DMAP; pyridine / CH₂Cl₂ / 3 h / 20 °C

2: 83 percent / Et₃SiH; CF₃CO₂H / CH₂Cl₂ / 1.5 h / 20 °C

3: 90 percent / t-butyldimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.5 h / -40 - 30 °C

4: 87 percent / TBAF / tetrahydrofuran / 2 h / 20 °C

With pyridine; triethylsilane; dmap; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0713335

Reference yield:

: C₃₀H₄₂O₇Si

: 949159-01-7
C₄₅H₅₀O₁₃

Guidance literature:: Multi-step reaction with 3 steps

1: TMSOTf / CH₂Cl₂ / -40 °C

2: 90 percent / t-butyldimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 0.5 h / -40 - 30 °C

3: 87 percent / TBAF / tetrahydrofuran / 2 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; t-butyldimethylsiyl triflate; tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0713335