(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

Base Information

Chemical Name:(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran
CAS No.:283147-88-6
Molecular Formula:C₅₅H₆₀O₉S
Molecular Weight:897.142
Hs Code.:

(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

Synonyms:(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

There total 3 articles about (2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39483-51-7,119645-03-3,126461-54-9,128850-50-0
ethyl 2,3,4-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 2-((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-sulfonyl)-pyridine

: (2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2R,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

: 283147-88-6
(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

Guidance literature:: With samarium(III) trifluoromethanesulfonate; In toluene; at 70 ℃;
DOI:10.1021/ol005579k

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 283147-88-6
(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / n-Bu₃P / CH₂Cl₂ / 2 h / 20 °C

2: 75 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 4 h / 20 °C

3: Sm(OTf)3 / toluene / 70 °C

With tributylphosphine; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; samarium(III) trifluoromethanesulfonate; In dichloromethane; toluene; 1: Substitution / 2: Oxidation / 3: Substitution;
DOI:10.1021/ol005579k

Reference yield:

: 205485-61-6
2-((3S,4R,5R)-3,4-Bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-ylsulfanyl)-pyridine

: 283147-88-6
(2R,3R,4S,5S,6R)-3,4,5-Tris-benzyloxy-2-((2S,3S,4R,5R)-3,4-bis-benzyloxy-5-benzyloxymethyl-tetrahydro-furan-2-yloxymethyl)-6-ethylsulfanyl-tetrahydro-pyran

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / m-CPBA; NaHCO₃ / CH₂Cl₂ / 4 h / 20 °C

2: Sm(OTf)3 / toluene / 70 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; samarium(III) trifluoromethanesulfonate; In dichloromethane; toluene; 1: Oxidation / 2: Substitution;
DOI:10.1021/ol005579k