Technology Process of C25H25N5O4
There total 3 articles about C25H25N5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 18h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride;
In
tetrahydrofuran; 1,4-dioxane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium acetate; palladium diacetate / 1,4-dioxane / 18 h / 100 °C / Inert atmosphere
2: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; potassium acetate; palladium diacetate;
In
tetrahydrofuran; 1,4-dioxane; water;