C₂₅H₂₇NO₆

Base Information

Chemical Name:C₂₅H₂₇NO₆
CAS No.:1265278-80-5
Molecular Formula:C₂₅H₂₇NO₆
Molecular Weight:437.492
Hs Code.:

C<sub>25</sub>H<sub>27</sub>NO<sub>6</sub>

Synonyms:C₂₅H₂₇NO₆

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Chemical Property of C₂₅H₂₇NO₆

Chemical Property:

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Technology Process of C₂₅H₂₇NO₆

There total 22 articles about C₂₅H₂₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1265279-47-7
C₃₀H₃₉NO₆Si

: 1265278-80-5
C₂₅H₂₇NO₆

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; HATU; In N,N-dimethyl-formamide; at 23 - 40 ℃; for 1.33333h; Inert atmosphere;
DOI:10.1002/ejoc.201001281

Reference yield:

: 1048970-79-1
C₂₉H₃₄O₃Si

: 1265278-80-5
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 16 steps

1.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

3.1: [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate / 0.5 h / 0 - 23 °C / Inert atmosphere

4.1: Trimethyl borate / toluene / 16.3 h / 23 °C / Inert atmosphere; Reflux

5.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C

6.1: pyridinium chlorochromate / dichloromethane / 16 h / 23 °C / Inert atmosphere; Molecular sieve

7.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - 0 °C / Inert atmosphere

8.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 16 h / 23 - 78 °C / Inert atmosphere

9.1: methanol; samarium diiodide / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

10.1: tetrahydrofuran / 0.5 h / 0 - 23 °C / Inert atmosphere

11.1: tert.-butylhydroperoxide / decane; ethyl acetate / 0.5 h / 23 °C / Inert atmosphere; Molecular sieve

11.2: 16 h / 23 °C / Inert atmosphere

12.1: Martins sulfurane / dichloromethane / 2 h / 23 °C / Inert atmosphere

13.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

13.2: 3 h / -78 - 0 °C / Inert atmosphere

14.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.58 h / -78 °C / Inert atmosphere

14.2: 3 h / -78 - 0 °C / Inert atmosphere

15.1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

16.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride; HATU / N,N-dimethyl-formamide / 1.33 h / 23 - 40 °C / Inert atmosphere

With methanol; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; bis-triphenylphosphine-palladium(II) chloride; formic acid; Hoveyda-Grubbs catalyst second generation; samarium diiodide; Martins sulfurane; Trimethyl borate; tributyl-amine; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; hydrogen; potassium hexamethylsilazane; potassium hydrogencarbonate; HATU; pyridinium chlorochromate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; decane; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene; 1.1: Corey-Bakshi-Shibata reduction / 4.1: Intramolecular Diels-Alder reaction;
DOI:10.1002/ejoc.201001281

Reference yield:

: 108534-61-8
(2-methoxyphenoxy)-(1,1-dimethylethyl)diphenylsilane

: 1265278-80-5
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 17 steps

1.1: N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium / diethyl ether; cyclohexane / 0.75 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 °C / Inert atmosphere

2.1: (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

4.1: [bis(acetoxy)iodo]benzene; potassium hydrogencarbonate / 0.5 h / 0 - 23 °C / Inert atmosphere

5.1: Trimethyl borate / toluene / 16.3 h / 23 °C / Inert atmosphere; Reflux

6.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 23 °C

7.1: pyridinium chlorochromate / dichloromethane / 16 h / 23 °C / Inert atmosphere; Molecular sieve

8.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 - 0 °C / Inert atmosphere

9.1: bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine / N,N-dimethyl-formamide / 16 h / 23 - 78 °C / Inert atmosphere

10.1: methanol; samarium diiodide / tetrahydrofuran / 0.33 h / 23 °C / Inert atmosphere

11.1: tetrahydrofuran / 0.5 h / 0 - 23 °C / Inert atmosphere

12.1: tert.-butylhydroperoxide / decane; ethyl acetate / 0.5 h / 23 °C / Inert atmosphere; Molecular sieve

12.2: 16 h / 23 °C / Inert atmosphere

13.1: Martins sulfurane / dichloromethane / 2 h / 23 °C / Inert atmosphere

14.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.5 h / -78 °C / Inert atmosphere

14.2: 3 h / -78 - 0 °C / Inert atmosphere

15.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.58 h / -78 °C / Inert atmosphere

15.2: 3 h / -78 - 0 °C / Inert atmosphere

16.1: Hoveyda-Grubbs catalyst second generation / benzene / 1.17 h / 70 °C / Inert atmosphere

17.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride; HATU / N,N-dimethyl-formamide / 1.33 h / 23 - 40 °C / Inert atmosphere

With methanol; tert.-butylhydroperoxide; N,N,N,N,N,N-hexamethylphosphoric triamide; bis-triphenylphosphine-palladium(II) chloride; formic acid; Hoveyda-Grubbs catalyst second generation; samarium diiodide; Martins sulfurane; Trimethyl borate; tributyl-amine; N,N,N,N,-tetramethylethylenediamine; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; hydrogen; sec.-butyllithium; potassium hexamethylsilazane; potassium hydrogencarbonate; HATU; pyridinium chlorochromate; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole; In tetrahydrofuran; methanol; diethyl ether; decane; dichloromethane; cyclohexane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene; 2.1: Corey-Bakshi-Shibata reduction / 5.1: Intramolecular Diels-Alder reaction;
DOI:10.1002/ejoc.201001281