C₁₄H₂₀O₂S

Base Information

• Chemical Name: C₁₄H₂₀O₂S
• CAS No.: 1356965-41-7
• Molecular Formula: C₁₄H₂₀O₂S
• Molecular Weight: 252.378
• Mol file: 1356965-41-7.mol

Synonyms:C₁₄H₂₀O₂S

Chemical Property of C₁₄H₂₀O₂S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₂₀O₂S

There total 3 articles about C₁₄H₂₀O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C14H20S (1356965-79-1) → C14H20O2S (1356965-41-7)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1021/ja210758n

Reference yield:

C18H29O4PS (1356965-48-4) → C14H20O2S (1356965-41-7)

Guidance literature:

Multi-step reaction with 3 steps

1: borane-THF; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 0 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

With borane-THF; sodium hydride; 3-chloro-benzenecarboperoxoic acid; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja210758n

Reference yield:

C18H31O4PS (1356965-64-4) → C14H20O2S (1356965-41-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 55 °C / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 5 h / 20 °C / Inert atmosphere

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ja210758n

upstream raw materials:

C₁₈H₃₁O₄PS

C₁₄H₂₀S

C₁₈H₂₉O₄PS