(E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Base Information

Chemical Name:(E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene
CAS No.:340157-83-7
Molecular Formula:C₁₄H₆BrF₁₃
Molecular Weight:501.085
Hs Code.:

Synonyms:(E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

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MSDS Files:: SDS file from LookChem

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Technology Process of (E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

There total 4 articles about (E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene

: 673-40-5
4-bromobenzenediazonium tetrafluoroborate

: 340157-83-7
(E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Guidance literature:: With palladium diacetate; In methanol; at 40 ℃; for 0.166667h;
DOI:10.1002/1099-0690(200103)2001:6<1121::AID-EJOC1121>3.0.CO;2-3

Reference yield: 91.0%

: 589-87-7
1,4-bromoiodobenzene

: 25291-17-2
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene

: 340157-83-7
(E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Guidance literature:: With tetrabutylammomium bromide; sodium acetate; palladium diacetate; In N,N-dimethyl-formamide; at 110 ℃; for 24h;
DOI:10.1016/S0040-4039(01)00714-6

Reference yield: 71.0%

: 335-56-8
1-bromo-1,1,2,2,3,3,4,4,5,5,6,6,6-tridecafluorohexane

: 1200-07-3
3-(4-bromophenyl)acrylic acid

: 340157-83-7
(E)-1-bromo-4-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octen-1-yl)benzene

Guidance literature:: With [2,2]bipyridinyl; copper(I) trifluoromethanesolfonate toluene complex; Dimethyl phosphite; In acetonitrile; at 80 ℃; for 72h; stereoselective reaction; Schlenk technique; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.6b02613