methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

Base Information

Chemical Name:methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide
CAS No.:166322-27-6
Molecular Formula:C₂₃H₂₇NO₃
Molecular Weight:365.472
Hs Code.:

Synonyms:methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

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Chemical Property of methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

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Technology Process of methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

There total 3 articles about methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 132991-63-0
methyl 4-<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalen-2-yl)aminomethyl>-benzoate

: 166322-27-6
methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In acetone; at 0 ℃; for 0.5h;
DOI:10.1080/00397919508011829

Reference yield:

: 92050-16-3
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthylamine

: 166322-27-6
methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaBH₃CN, AcOH / methanol / 0.08 h

2: 67 percent / MCPBA / acetone / 0.5 h / 0 °C

With sodium cyanoborohydride; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; acetone;
DOI:10.1080/00397919508011829

Reference yield:

: 1571-08-0
methyl 4-formylbenzoate

: 166322-27-6
methyl 4-<<(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-naphthalene)-2-imino>methylene>-benzoate, N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaBH₃CN, AcOH / methanol / 0.08 h

2: 67 percent / MCPBA / acetone / 0.5 h / 0 °C

With sodium cyanoborohydride; acetic acid; 3-chloro-benzenecarboperoxoic acid; In methanol; acetone;
DOI:10.1080/00397919508011829