N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide

Base Information

Chemical Name:N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide
CAS No.:1374154-93-4
Molecular Formula:C₁₈H₂₁NO₆S₂
Molecular Weight:411.5
Hs Code.:

Synonyms:N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide

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Chemical Property of N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide

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Technology Process of N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide

There total 2 articles about N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 63758-12-3
6-chlorosulfonyl-1,4-benzodioxane

: 959252-70-1
N-ethyl-N-(m-tolyl)methanesulfonamide

: 1374154-93-4
N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide

Guidance literature:: 6-chlorosulfonyl-1,4-benzodioxane; aluminum (III) chloride; In 1,1-dichloroethane; for 0.166667h;

N-ethyl-N-(m-tolyl)methanesulfonamide; In 1,1-dichloroethane; at 70 ℃; Pressure ampoule;

Reference yield:

: 102-27-2
N-ethyl-m-toulidine

: 1374154-93-4
N-(4-((2,3-dihydrobenzo[b][1,4]dioxin-6-yl)sulfonyl)-3-methylphenyl)-N-ethylmethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 20 °C

2.1: aluminum (III) chloride / 1,1-dichloroethane / 0.17 h

2.2: 70 °C / Pressure ampoule

With pyridine; aluminum (III) chloride; In 1,1-dichloroethane; 2.2: Friedel Crafts Acylation;