C₁₇H₂₂O₄S

Base Information

Chemical Name:C₁₇H₂₂O₄S
CAS No.:1274905-59-7
Molecular Formula:C₁₇H₂₂O₄S
Molecular Weight:322.425
Hs Code.:

C<sub>17</sub>H<sub>22</sub>O<sub>4</sub>S

Synonyms:C₁₇H₂₂O₄S

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Chemical Property of C₁₇H₂₂O₄S

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Technology Process of C₁₇H₂₂O₄S

There total 5 articles about C₁₇H₂₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: C₁₇H₂₂O₄S

: 1274905-59-7
C₁₇H₂₂O₄S

Guidance literature:: With camphor-10-sulfonic acid; In 1,2-dichloro-ethane; at 70 ℃; for 10.5h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol200333p

Reference yield:

: 1274905-71-3
C₉H₁₆O₃

: 872827-92-4
S-(4-methylphenyl) 2-propenethioate

: 1274905-59-7
C₁₇H₂₂O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 18 h / 35 °C / Inert atmosphere

2: camphor-10-sulfonic acid / 1,2-dichloro-ethane / 10.5 h / 70 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; camphor-10-sulfonic acid; In dichloromethane; 1,2-dichloro-ethane; 2: oxa Michael cyclization;
DOI:10.1021/ol200333p

Reference yield:

: 125877-83-0
(2'S,3'S)-3'-(tert-butyldimethylsiloxy)-tetrahydropyran-2'-carbaldehyde

: 1274905-59-7
C₁₇H₂₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran; diethyl ether / 0.83 h / 0 °C / Inert atmosphere

2: (1S)-10-camphorsulfonic acid / methanol / 6.5 h / 20 °C / Inert atmosphere

3: Hoveyda-Grubbs catalyst second generation / dichloromethane / 18 h / 35 °C / Inert atmosphere

4: (1S)-10-camphorsulfonic acid / 1,2-dichloro-ethane / 10.5 h / 70 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; (1S)-10-camphorsulfonic acid; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jo202179s