2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

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Chemical Name:2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide
CAS No.:474903-38-3
Molecular Formula:C₅₂H₆₇N₅O₁₆
Molecular Weight:1018.13
Hs Code.:

2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

Synonyms:2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

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Chemical Property of 2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

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Technology Process of 2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

There total 2 articles about 2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 169744-02-9
{2-[2-(2-amino-ethoxy)-ethoxy]-ethyl}-carbamic acid benzyl ester

: 474903-35-0
2-oxoethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

: 474903-38-3
2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

Guidance literature:: With sodium cyanoborohydride; In methanol; at 20 ℃; for 18h; pH=7;
DOI:10.1016/S0040-4020(02)00838-4

Reference yield:

: allyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

: 474903-38-3
2-(2-{2-[2-(benzyloxycarbonylamino)ethoxy]ethoxy}ethylamino)ethyl 2-O-(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-3-O-carbamoyl-α-D-galactopyranosiduronamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: O₃ / methanol / 0.08 h / -78 °C

1.2: 94 percent / dimethylsulfide

2.1: 76 percent / sodium cyanoborohydride / methanol / 18 h / 20 °C / pH 7

With sodium cyanoborohydride; ozone; In methanol;
DOI:10.1016/S0040-4020(02)00838-4