N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline

Base Information

• Chemical Name: N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline
• CAS No.: 371192-45-9
• Molecular Formula: C₁₆H₂₀ClNO
• Molecular Weight: 277.794
• Mol file: 371192-45-9.mol

Synonyms:N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline

Chemical Property of N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline

There total 2 articles about N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-methacryloyl-2-(cyclopent-1-enyl)-6-methylaniline (371192-33-5) → N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline (371192-45-9)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 0.166667h;

DOI:10.1023/A:1011312912357

Reference yield:

6-(cyclopent-1-en-1-yl)-2-methyl-aniline (235779-09-6) → N-(3-chloro-2-methylpropanoyl)-6-(cyclopent-1-enyl)-2-methylaniline (371192-45-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / K₂CO₃ / CH₂Cl₂ / 1.5 h / 20 °C

2: 70 percent / HCl(g) / CH₂Cl₂ / 0.17 h / 20 °C

With hydrogenchloride; potassium carbonate; In dichloromethane;

DOI:10.1023/A:1011312912357

upstream raw materials:

N-methacryloyl-2-(cyclopent-1-enyl)-6-methylaniline

6-(cyclopent-1-en-1-yl)-2-methyl-aniline