<2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Base Information

Chemical Name:<2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid
CAS No.:103148-86-3
Molecular Formula:C₂₉H₂₇NOP*Cl
Molecular Weight:471.966
Hs Code.:

Synonyms:<2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Suppliers and Price of <2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of <2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of <2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

There total 3 articles about <2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 28668-58-8
1-(α-chloroacetyl)-1,2,3,4-tetrahydroquinoline

: 603-35-0
triphenylphosphine

: 103148-86-3
<2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Guidance literature:: In toluene; for 24h; Heating;

Reference yield:

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 103148-86-3
<2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / pyridine / toluene / 12 h / Ambient temperature

2: 65 percent / toluene / 24 h / Heating

With pyridine; In toluene;

Reference yield:

: 635-46-1
1,2,3,4-tetrahydroisoquinoline

: 103148-86-3
<2-Oxo-2-(1,2,3,4-tetrahydro-1-chinolinyl)ethyl>triphenylphosphoniumchlorid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 3.5 h / 0 - 20 °C

2: toluene / 30 h / Reflux

With potassium carbonate; In acetone; toluene;
DOI:10.1055/s-0032-1317703