N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

Base Information

Chemical Name:N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide
CAS No.:911210-71-4
Molecular Formula:C₅₀H₆₀N₄O₁₀S₂
Molecular Weight:941.179
Hs Code.:

N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

Synonyms:N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

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Chemical Property of N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

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Technology Process of N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

There total 3 articles about N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 911210-72-5
5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-ol

: 3559-06-6
toluene-4-sulfonic acid 2-[methyl-(toluene-4-sulfonyl)-amino]-ethyl ester

: 911210-71-4
N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

Guidance literature:: 5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-ol; toluene-4-sulfonic acid 2-[methyl-(toluene-4-sulfonyl)-amino]-ethyl ester; With sodium hydride; In tetrahydrofuran; at 20 - 45 ℃; for 72h;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 911210-71-4
N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 h / 0 - 20 °C

2: sodium hydride / tetrahydrofuran / 72 h / 20 - 45 °C

With sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]piperidin-3-ol

: 98-59-9
p-toluenesulfonyl chloride

: 911210-71-4
N-{2-[5-[4-(3-methoxypropyl)-3,4-dihydro-2H-benzo[1,4]oxazin-6-ylmethoxy]-4-[4-(4-methyl-3,4-dihydro-2H-benzo[1,4]oxazin-7-yloxy)phenyl]-1-(toluene-4-sulphonyl)piperidin-3-yloxy]ethyl}-4,N-dimethylbenzenesulphonamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / water; ethyl acetate / 15 h

2: sodium hydride / tetrahydrofuran / 72 h / 20 - 45 °C

With sodium hydride; sodium carbonate; In tetrahydrofuran; water; ethyl acetate;