2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one

Base Information

• Chemical Name: 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one
• CAS No.: 31568-62-4
• Molecular Formula: C₂₇H₃₂N₂O₃S
• Molecular Weight: 464.629

Synonyms:2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one

Chemical Property of 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one

Chemical Property:

Purity/Quality:

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Technology Process of 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one

There total 4 articles about 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

2,6-Di-tert-butyl-1,4-benzoquinone (719-22-2) + N-tosyl-1,2-diaminobenzene (3624-90-6) → 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one (31568-62-4)

Guidance literature:

In isopropyl alcohol; Heating;

DOI:10.1023/A:1012399922502

Reference yield:

1,2-diamino-benzene (95-54-5) → 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one (31568-62-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / pyridine / tetrahydrofuran / 20 °C

2: 50 percent / propan-2-ol / Heating

With pyridine; In tetrahydrofuran; isopropyl alcohol;

DOI:10.1023/A:1012399922502

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → 2,6-di-tert-butyl-4--2,5-cyclohexadien-1-one (31568-62-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / pyridine / tetrahydrofuran / 20 °C

2: 50 percent / propan-2-ol / Heating

With pyridine; In tetrahydrofuran; isopropyl alcohol;

DOI:10.1023/A:1012399922502

upstream raw materials:

2,6-Di-tert-butyl-1,4-benzoquinone

N-tosyl-1,2-diaminobenzene

1,2-diamino-benzene

p-toluenesulfonyl chloride

Downstream raw materials:

{Ni(C₆H₂(O)(C(CH₃)3)2NC₆H₄NSO₂C₆H₄CH₃)2}

{Pd(C₆H₂(O)(C(CH₃)3)2NC₆H₄NSO₂C₆H₄CH₃)2}

bis{2,6-di-tert-butyl-4-{o-(tosylamino)-phenylimino}-2,5-cyclohexadien-1-one}-zinc(II)

bis{2,6-di-tert-butyl-4-{o-(tosylamino)-phenylimino}-2,5-cyclohexadien-1-one}-cadmium(II)

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