N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide

Base Information

Chemical Name:N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide
CAS No.:1440762-42-4
Molecular Formula:C₄₃H₃₆F₃N₃O₅
Molecular Weight:731.771
Hs Code.:

Synonyms:N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide

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Chemical Property of N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide

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Technology Process of N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide

There total 2 articles about N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1294450-29-5
N,N’-bis(1-ethylpropyl)-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)perylene-3,4:9,10-tetracarboxylic acid bisimide

: 175135-49-6
N-(2-bromo-4-(trifluoromethyl)phenyl)acetamide

: 1440762-42-4
N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide

Guidance literature:: With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium carbonate; In water; toluene; for 24h; Inert atmosphere; Reflux; Schlenk technique;
DOI:10.1021/ol401316q

Reference yield:

: 110590-81-3
N,N'-bis(1-ethylpropyl)-3,4:9,10-perylenebis(dicarboximide)

: 1440762-42-4
N,N’-bis(1-ethylpropyl)-2-(4-trifluoromethylacetanilide-2-yl)perylene-3,4:9,10-tetracarboxylicacid bisimide

Guidance literature:: Multi-step reaction with 2 steps

1: tris(pentafluorophenyl)phosphine; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer / 1,4-dioxane / 24 h / 110 °C / Inert atmosphere

2: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; potassium carbonate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / toluene; water / 24 h / Inert atmosphere; Reflux; Schlenk technique

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; potassium carbonate; tris(pentafluorophenyl)phosphine; In 1,4-dioxane; water; toluene; 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol401316q