C₃₃H₄₂N₂O₈

Base Information

Chemical Name:C₃₃H₄₂N₂O₈
CAS No.:1009094-24-9
Molecular Formula:C₃₃H₄₂N₂O₈
Molecular Weight:594.705
Hs Code.:

C<sub>33</sub>H<sub>42</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:C₃₃H₄₂N₂O₈

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Chemical Property of C₃₃H₄₂N₂O₈

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Technology Process of C₃₃H₄₂N₂O₈

There total 7 articles about C₃₃H₄₂N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1009094-23-8
C₃₃H₄₂N₂O₇

: 1009094-24-9
C₃₃H₄₂N₂O₈

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; at 20 ℃; for 0.833333h;

Reference yield:

: 874347-52-1
C₁₅H₁₈INO₅

: 1009094-24-9
C₃₃H₄₂N₂O₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

1.2: 20 °C

1.3: 2 h

2.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.08 h

2.2: 1 h / 70 °C

3.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran / 0.83 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; trimethylaluminum; potassium acetate; caesium carbonate; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 874347-50-9
C₈H₁₀INO₂

: 1009094-24-9
C₃₃H₄₂N₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzene / Heating / reflux

2.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

2.2: 2 h

3.1: pyridine hydrogenfluoride / tetrahydrofuran; pyridine / 4 h / 20 °C

4.1: trimethylaluminum / hexane; dichloromethane / 0.25 h

4.2: 20 °C

4.3: 2 h

5.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.08 h

5.2: 1 h / 70 °C

6.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / tetrahydrofuran / 0.83 h / 20 °C

With titanium(IV) isopropylate; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; trimethylaluminum; potassium acetate; caesium carbonate; pyridine hydrogenfluoride; In tetrahydrofuran; pyridine; hexane; dichloromethane; dimethyl sulfoxide; toluene; benzene;