1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Base Information

Chemical Name:1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione
CAS No.:84212-57-7
Molecular Formula:C₂₀H₂₂O₈
Molecular Weight:390.39
Hs Code.:

Synonyms:1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Suppliers and Price of 1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

There total 4 articles about 1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 121817-16-1
2-acetyl-3,5-dimethoxyphenyl-3,4,5-trimethoxyphenyl ester

: 84212-57-7
1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Guidance literature:: With pyridine; sodium hydroxide; at 50 ℃; for 2h; Inert atmosphere;

Reference yield:

: 90-24-4
2-hydroxy-4,6-dimethoxyacetophenone

: 84212-57-7
1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 110 °C

2: pyridine; potassium hydroxide / 4 h / 60 °C

With pyridine; potassium hydroxide; 2: |Baker-Venkataraman Rearrangement;
DOI:10.3390/molecules19078933

Reference yield:

: 480-66-0,67471-34-5
2,4,6-trihydroxyacetophenone

: 84212-57-7
1-(4,6-dimethoxy-2-hydroxyphenyl)-3-(3,4,5-trimethoxyphenyl)propan-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / 16 h / 20 °C

2: potassium carbonate / acetone / 24 h / 20 °C / Inert atmosphere

3: pyridine; sodium hydroxide / 2 h / 50 °C / Inert atmosphere

With pyridine; potassium carbonate; sodium hydroxide; In acetone; 3: |Baker-Venkataraman Rearrangement;