(2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

Base Information

Chemical Name:(2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid
CAS No.:120554-40-7
Molecular Formula:C₁₇H₂₂O₃
Molecular Weight:274.36
Hs Code.:

Synonyms:(2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

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Technology Process of (2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

There total 4 articles about (2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6397-82-6
4'-methoxyhexanophenone

: 120554-40-7
(2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi, (i-Pr)2NH / 1.) THF, hexane, -70 deg C, 5 min, 2.) THF, -70 -> -35 deg C, 15 min

3: 2.) NaOH / 1.) CH₂Cl₂, room temperature, 3 d, 2.) MeOH, H₂O, reflux, 30 min

With sodium hydroxide; n-butyllithium; diisopropylamine;
DOI:10.1021/jm00128a026

Reference yield:

: 120556-12-9
(R,S)-3-hydroxy-3-(4-methoxyphenyl)octanenitrile

: 120554-40-7
(2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

Guidance literature:: Multi-step reaction with 2 steps

2: 2.) NaOH / 1.) CH₂Cl₂, room temperature, 3 d, 2.) MeOH, H₂O, reflux, 30 min

With sodium hydroxide;
DOI:10.1021/jm00128a026

Reference yield:

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 120553-88-0
(Z)-3-(4-methoxyphenyl)-2-octenal

: 120554-40-7
(2E,4Z)-5-(4-methoxyphenyl)-2,4-decadienoic acid

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 3 d, 2.) MeOH, H₂O, reflux, 30 min;
DOI:10.1021/jm00128a026