11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

Base Information

Chemical Name:11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester
CAS No.:868836-33-3
Molecular Formula:C₅₉H₈₇N₅O₁₁S₄
Molecular Weight:1170.63
Hs Code.:

11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

Synonyms:11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

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Chemical Property of 11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

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Technology Process of 11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

There total 5 articles about 11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: C₅₂H₇₇N₅O₈S₄

: 35444-44-1
methyl adipoyl chloride

: 868836-33-3
11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm0505009

Reference yield: 74.0%

: 868836-33-3
11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

Guidance literature:

Reference yield:

: 868836-27-5
1-(phthalimido)-4,8,12-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-15-N-[2,4,6-(trimethyl)benzenesulfonylamino]-4,8,12-triazapentadecane

: 868836-33-3
11,15,19-tris{N-[2,4,6-(trimethyl)benzenesulfonyl]}-22-{N-[2,4,6-(trimethyl)benzenesulfonyl]-N-[(cyclopropyl)methyl]amino}-6-oxo-7,11,15,19-tetraazadocosanoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaH / dimethylformamide / 0 °C

1.2: 73 percent / dimethylformamide

2.1: hydrazine / methanol / 12 h / Heating

3.1: 74 percent / triethylamine / CH₂Cl₂ / 0 - 20 °C

With sodium hydride; triethylamine; hydrazine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm0505009