4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole

Base Information

Chemical Name:4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole
CAS No.:114155-44-1
Molecular Formula:C₁₆H₂₇BIPSi
Molecular Weight:416.165
Hs Code.:

Synonyms:4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole

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Chemical Property of 4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole

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Technology Process of 4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole

There total 2 articles about 4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 114130-48-2
dimeric (P-B)⁽²⁾-4,5-diethyl-2,5-dihydro-2,2,3-trimethyl-1-phenyl-1,2,5-phosphasilaborole

: 114155-44-1
4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole

Guidance literature:: With methyl iodide; In neat (no solvent); Ar atmosphere, refluxing (12 h, ca. 45°C); filtn., concn. (vacuum); elem. anal.;

Reference yield:

: 107098-30-6
(E)-ClSi(CH₃)2C(CH₃)C(C₂H₅)B(C₂H₅)Cl

: 114155-44-1
4,5-diethyl-2,5-dihydro-1,2,2,3-tetramethyl-1-phenyl-1,2,5-phosphoniasilaboratole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: methyl iodide / neat (no solvent)

With methyl iodide; In tetrahydrofuran;