PhC(Nt-Bu)2SiH(BH₃)

Base Information

• Chemical Name: PhC(Nt-Bu)2SiH(BH₃)
• CAS No.: 1309874-23-4
• Molecular Formula: C₁₅H₂₇BN₂Si
• Molecular Weight: 274.289

Synonyms:PhC(Nt-Bu)2SiH(BH₃)

Chemical Property of PhC(Nt-Bu)2SiH(BH₃)

Chemical Property:

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Technology Process of PhC(Nt-Bu)2SiH(BH₃)

There total 2 articles about PhC(Nt-Bu)2SiH(BH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

PhC(N-t-Bu)2SiCl(BH3) (1308663-40-2) → PhC(Nt-Bu)2SiH(BH3) (1309874-23-4)

Guidance literature:

With potassium tri-sec-butyl-borohydride; In tetrahydrofuran; at -30 - 20 ℃; Inert atmosphere;

DOI:10.1039/c0dt01675f

Reference yield: 65.0%

PhC(N-t-Bu)2SiCl(BH3) (1308663-40-2) + potassium tri-sec-butyl-borohydride → PhC(Nt-Bu)2SiH(BH3) (1309874-23-4)

Guidance literature:

In tetrahydrofuran; (N2) soln. potassium selectride in THF was added dropwise at -30°C to soln. complex in toluene, warmed to room temp. and stirred for 2 h; volatiles were removed, residue was extd. with toluene, crystn. from b-hexane; elem. anal.;

DOI:10.1039/c0dt01675f

upstream raw materials:

PhC(N-t-Bu)2SiCl(BH₃)

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