ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

Base Information

Chemical Name:ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate
CAS No.:1407969-05-4
Molecular Formula:C₆₂H₈₃NO₁₀
Molecular Weight:1002.34
Hs Code.:

ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

Synonyms:ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

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Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

There total 4 articles about ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1407969-04-3
C₄₆H₆₆O₇

: 238420-42-3
3-(benzyloxy)-1-(2-(2-iodoethoxy)ethyl)pyridin-2(1H)-one

: 1407969-05-4
ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

Guidance literature:: With caesium carbonate; In acetonitrile; for 16h; Reflux;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 1407968-94-8
4-tert-butyl-2-(5-tert-butyl-2-(tert-butyldiphenylsilyloxy)benzyl)-6-(5-tert-butyl-2-hydroxybenzyl)phenol

: 1407969-05-4
ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / acetonitrile / 72 h / Reflux

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

3: caesium carbonate / acetonitrile / 16 h / Reflux

With tetrabutyl ammonium fluoride; caesium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tet.2012.09.032

Reference yield:

: 1407969-03-2
ethyl 5-(4-tert-butyl-2-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)-6-(5-tertbutyl-2-(tert-butyldiphenylsilyloxy)benzyl)phenoxy)pentanoate

: 1407969-05-4
ethyl 5-(2-(2-(2-(2-(3-(benzyloxy)-2-oxopyridin-1(2H)-yl)ethoxy)ethoxy)-5-tertbutylbenzyl)-4-tert-butyl-6-(5-tert-butyl-2-(5-ethoxy-5-oxopentyloxy)benzyl)phenoxy)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C

2: caesium carbonate / acetonitrile / 16 h / Reflux

With tetrabutyl ammonium fluoride; caesium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tet.2012.09.032