3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Base Information

Chemical Name:3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate
CAS No.:884646-77-9
Molecular Formula:C₁₇H₁₆ClNO₈
Molecular Weight:397.769
Hs Code.:

Synonyms:3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Suppliers and Price of 3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

There total 7 articles about 3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 884646-76-8
3-formamido-6-methoxy-2,5-bis(methoxymethoxy)phenethyl 5-chloro-2,4-dihydroxybenzoate

: 884646-77-9
3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Guidance literature:: With chloro-trimethyl-silane; sodium iodide;

Reference yield:

: 884646-90-6
2-(2-methoxy-3,6-bis(methoxymethoxy)phenyl)ethanol

: 884646-77-9
3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: NH₄NO₃; (CF₃CO)2O / tetrahydrofuran / 0.25 h / 20 °C

1.2: 61 percent / LiOH / tetrahydrofuran; methanol; H₂O / 0.08 h

2.1: 51 percent / DMAP; DCC / dimethylformamide; tetrahydrofuran / 12 h / 50 °C

3.1: 85 percent / H₂ / PtO₂ / ethanol / 12 h / 20 °C

4.1: 91 percent / CH₂Cl₂ / 12 h / 30 °C

5.1: 86 percent / NaI; Me₃SiCl / CH₂Cl₂; acetonitrile / 0.25 h / 25 °C

With ammonium nitrate; dmap; chloro-trimethyl-silane; hydrogen; dicyclohexyl-carbodiimide; trifluoroacetic anhydride; sodium iodide; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo061054f

Reference yield:

: 884646-73-5
2-(2-methoxy-3,6-bis(methoxymethoxy)-5-nitrophenyl)ethanol

: 884646-77-9
3-formamido-2,5-dihydroxy-6-methoxyphenethyl 5-chloro-2,4-dihydroxybenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / DMAP; DCC / dimethylformamide; tetrahydrofuran / 12 h / 50 °C

2: 85 percent / H₂ / PtO₂ / ethanol / 12 h / 20 °C

3: 91 percent / CH₂Cl₂ / 12 h / 30 °C

4: 86 percent / NaI; Me₃SiCl / CH₂Cl₂; acetonitrile / 0.25 h / 25 °C

With dmap; chloro-trimethyl-silane; hydrogen; dicyclohexyl-carbodiimide; sodium iodide; platinum(IV) oxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo061054f