2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

Base Information

Chemical Name:2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside
CAS No.:791820-33-2
Molecular Formula:C₇₂H₁₀₉NO₁₁
Molecular Weight:1164.66
Hs Code.:

Synonyms:2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

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Chemical Property of 2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

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Technology Process of 2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

There total 4 articles about 2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 150-76-5
4-methoxy-phenol

: 791820-32-1
2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranoside

: 791820-33-2
2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 17h; Heating;
DOI:10.1081/CAR-200030039

Reference yield:

: 167612-35-3
2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 791820-33-2
2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves 4 Angstroem; N-iodosuccinimide; trimethylsilyl trifluoromethanesulfonate / benzene / 2 h / 7 °C

2: 82.8 mg / acetic acid / H₂O / 48 h / 45 °C

3: 88 percent / triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 17 h / Heating

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; benzene;
DOI:10.1081/CAR-200030039

Reference yield:

: N-[(4aR,6R,7R,8R,8aS)-8-Hydroxy-2-phenyl-6-(2-tetradecyl-hexadecyloxy)-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl]-acetamide

: 791820-33-2
2-(tetradecyl)hexadecyl (2,3,4-tri-O-benzyl-α-L-fucopyranosyl)-(1->3)-2-acetamido-2-deoxy-6-O-4-methoxyphenyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: molecular sieves 4 Angstroem; N-iodosuccinimide; trimethylsilyl trifluoromethanesulfonate / benzene / 2 h / 7 °C

2: 82.8 mg / acetic acid / H₂O / 48 h / 45 °C

3: 88 percent / triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 17 h / Heating

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; benzene;
DOI:10.1081/CAR-200030039