2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate
CAS No.:1228757-59-2
Molecular Formula:C₄₃H₄₂F₃NO₇
Molecular Weight:741.804
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Suppliers and Price of 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

There total 3 articles about 2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidoyl chloride

: 1228757-59-2
2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In N,N-dimethyl-formamide; for 2h; Reagent/catalyst;
DOI:10.1039/c9ob02696g

Reference yield:

: 14815-12-4
N-(2-methoxyphenyl)-2,2,2-trifluoro-acetamide

: 1228757-59-2
2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrachloromethane; triphenylphosphine / dichloromethane / 4 h / 60 °C

2.1: 15-crown-5; sodium hydride / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

With tetrachloromethane; 15-crown-5; sodium hydride; triphenylphosphine; In dichloromethane;
DOI:10.1080/07328301003597673

Reference yield:

: 90-04-0
2-methoxy-phenylamine

: 1228757-59-2
2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl N-(2-methoxyphenyl)-2,2,2-trifluoroacetimidate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 3 h / 20 °C

2.1: tetrachloromethane; triphenylphosphine / dichloromethane / 4 h / 60 °C

3.1: 15-crown-5; sodium hydride / dichloromethane / 0.08 h / 20 °C / Inert atmosphere

3.2: 0.5 h / 20 °C / Inert atmosphere

With tetrachloromethane; 15-crown-5; sodium hydride; triphenylphosphine; In dichloromethane;
DOI:10.1080/07328301003597673