4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Base Information

Chemical Name:4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile
CAS No.:1311137-16-2
Molecular Formula:C₁₉H₁₈N₄O₃
Molecular Weight:350.377
Hs Code.:

Synonyms:4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Suppliers and Price of 4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

There total 6 articles about 4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4997-55-1
3-ethyl-4-hydroxy-benzonitrile

: 1311138-62-1
3-(6-fluoropyridin-3-yl)-5,5-dimethyl-imidazolidine-2,4-dione

: 1311137-16-2
4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 96h;

Reference yield:

: 317358-76-2
4-(benzyloxy)-3-bromobenzonitrile

: 1311137-16-2
4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc(II) chloride / tetrahydrofuran / 0.5 h / 0 °C

1.2: 0 - 20 °C

2.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; ethanol / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 96 h / 120 °C

With hydrogen; potassium carbonate; zinc(II) chloride; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 2315-86-8
3-bromo-4-hydroxybenzonitrile

: 1311137-16-2
4-{[5-(4,4-dimethyl-2,5-dioxo-1-imidazolidinyl)-2-pyridinyl]oxy}-3-ethylbenzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetone / 50 °C

2.1: zinc(II) chloride / tetrahydrofuran / 0.5 h / 0 °C

2.2: 0 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate; ethanol / 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 96 h / 120 °C

With hydrogen; potassium carbonate; zinc(II) chloride; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; ethyl acetate; N,N-dimethyl-formamide; acetone;