N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

Base Information

Chemical Name:N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide
CAS No.:873848-12-5
Molecular Formula:C₅₃H₇₁NO₁₇
Molecular Weight:994.143
Hs Code.:

N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

Synonyms:N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

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Chemical Property of N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

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Technology Process of N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

There total 7 articles about N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112-35-6,95507-80-5
triethylene glucol monomethyl ether

: 873848-12-5
N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / Et₃N / CH₂Cl₂

2: 78 percent / NaH / dimethylformamide

3: 100 percent / Et₃N / CH₂Cl₂

4: NaI; K₂CO₃ / 50 °C

5: aq. NaOH / dimethylformamide

6: triphosgene; collidine / tetrahydrofuran

With 2,3,5-trimethyl-pyridine; sodium hydroxide; bis(trichloromethyl) carbonate; sodium hydride; potassium carbonate; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-872269

Reference yield:

: 23783-42-8,95507-80-5
tetraethylene glycol monomethyl ether

: 873848-12-5
N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / Et₃N / CH₂Cl₂

2: NaI; K₂CO₃ / 50 °C

3: aq. NaOH / dimethylformamide

4: triphosgene; collidine / tetrahydrofuran

With 2,3,5-trimethyl-pyridine; sodium hydroxide; bis(trichloromethyl) carbonate; potassium carbonate; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-872269

Reference yield:

: 74654-05-0
8-methoxy-1-(methylsulfonyl)oxy-3,6-dioxaoctane

: 873848-12-5
N-[4-((2R,4aR,6S,7R,8S,8aR)-8-Benzyloxy-6-methoxy-2-phenyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yloxymethyl)-phenyl]-3,5-bis-(2-{2-[2-(2-methoxy-ethoxy)-ethoxy]-ethoxy}-ethoxy)-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / NaH / dimethylformamide

2: 100 percent / Et₃N / CH₂Cl₂

3: NaI; K₂CO₃ / 50 °C

4: aq. NaOH / dimethylformamide

5: triphosgene; collidine / tetrahydrofuran

With 2,3,5-trimethyl-pyridine; sodium hydroxide; bis(trichloromethyl) carbonate; sodium hydride; potassium carbonate; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2005-872269