C₄₃H₆₂O₄Si

Base Information

Chemical Name:C₄₃H₆₂O₄Si
CAS No.:1319725-92-2
Molecular Formula:C₄₃H₆₂O₄Si
Molecular Weight:671.048
Hs Code.:

C<sub>43</sub>H<sub>62</sub>O<sub>4</sub>Si

Synonyms:C₄₃H₆₂O₄Si

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Chemical Property of C₄₃H₆₂O₄Si

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Technology Process of C₄₃H₆₂O₄Si

There total 8 articles about C₄₃H₆₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1319726-05-0
C₃₇H₄₈O₄

: 69739-34-0
t-butyldimethylsiyl triflate

: 1319725-92-2
C₄₃H₆₂O₄Si

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c1ob05251a

Reference yield:

: 1319725-93-3
C₃₀H₄₂O₄

: 1319725-92-2
C₄₃H₆₂O₄Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxygen; palladium dichloride / N,N-dimethyl acetamide / 1 h / 20 °C / 9000.9 Torr

1.2: 12 h / 90 °C / 3000.3 Torr

2.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere

2.2: 0.75 h / -100 °C / Inert atmosphere

2.3: -100 - 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

4.1: sulfuric acid / 1,4-dioxane; water / 6 h / 20 °C / Reflux

5.1: potassium carbonate / methanol / 14 h / 20 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 2 h / 20 °C

With sulfuric acid; oxygen; sodium hydride; potassium carbonate; triethylamine; palladium dichloride; lithium iodide; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl acetamide; water; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05251a

Reference yield:

: 1319726-00-5
C₃₀H₄₂O₅

: 1319725-92-2
C₄₃H₆₂O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium iodide / diethyl ether / 0.17 h / -40 °C / Inert atmosphere

1.2: 0.75 h / -100 °C / Inert atmosphere

1.3: -100 - 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

3.1: sulfuric acid / 1,4-dioxane; water / 6 h / 20 °C / Reflux

4.1: potassium carbonate / methanol / 14 h / 20 °C / Inert atmosphere

5.1: triethylamine / dichloromethane / 2 h / 20 °C

With sulfuric acid; sodium hydride; potassium carbonate; triethylamine; lithium iodide; In 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1039/c1ob05251a