α,α'-di-O-methoxyphenoxy adepate de dimethyle

Base Information

• Chemical Name: α,α'-di-O-methoxyphenoxy adepate de dimethyle
• CAS No.: 128312-34-5
• Molecular Formula: C₂₂H₂₆O₈
• Molecular Weight: 418.444
• Mol file: 128312-34-5.mol

Synonyms:α,α'-di-O-methoxyphenoxy adepate de dimethyle

Chemical Property of α,α'-di-O-methoxyphenoxy adepate de dimethyle

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α,α'-di-O-methoxyphenoxy adepate de dimethyle

There total 4 articles about α,α'-di-O-methoxyphenoxy adepate de dimethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

dimethyl 2,5-dibromohexanedioate (868-72-4,53490-47-4,124819-17-6) + 2-methoxy-phenol (90-05-1) → α,α'-di-O-methoxyphenoxy adepate de dimethyle (128312-34-5)

Guidance literature:

With Tris(3,6-dioxaheptyl)amine; potassium carbonate; In toluene; at 75 ℃; for 14h;

Reference yield:

Adipic acid (124-04-9) → α,α'-di-O-methoxyphenoxy adepate de dimethyle (128312-34-5)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride

2: bromine / 2 h / Heating

3: Ambient temperature

4: 50 percent / K₂CO₃, tris(3,6-dioxaheptyl)amine / toluene / 14 h / 75 °C

With thionyl chloride; Tris(3,6-dioxaheptyl)amine; bromine; potassium carbonate; In toluene;

Reference yield:

2,5-dibromohexanedioyl dichloride (29548-86-5,137300-49-3) → α,α'-di-O-methoxyphenoxy adepate de dimethyle (128312-34-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Ambient temperature

2: 50 percent / K₂CO₃, tris(3,6-dioxaheptyl)amine / toluene / 14 h / 75 °C

With Tris(3,6-dioxaheptyl)amine; potassium carbonate; In toluene;

upstream raw materials:

dimethyl 2,5-dibromohexanedioate

2-methoxy-phenol

Adipic acid

2,5-dibromohexanedioyl dichloride

Downstream raw materials:

acide α,α'-di-O-methoxyphenoxy adipique

acide α,α'-di-O-hydroxyphenoxy adipique