methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

Base Information

Chemical Name:methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate
CAS No.:1226754-49-9
Molecular Formula:C₂HF₃O₂*C₁₄H₁₈ClNO₄
Molecular Weight:413.778
Hs Code.:

Synonyms:methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

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Chemical Property of methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

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Technology Process of methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

There total 1 articles about methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1154415-30-1
tert-butyl 4-[2-chloro-5-methoxy-4-(methoxycarbonyl)phenoxy]piperidine-1-carboxylate

: 1226754-49-9
methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

: 1226754-49-9
methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 5-chloro-4-[(1-formylpiperidin-4-yl)oxy]-2-methoxybenzamide

Guidance literature:: methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate; N,N-dimethyl-formamide; With sodium methylate; In methanol; at 80 ℃; for 3h;

With ammonium formate; In methanol; at 170 - 180 ℃; for 6h;

Reference yield:

: 1226754-49-9
methyl 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzoate trifluoroacetate

: 5-chloro-2-methoxy-4-(piperidin-4-yloxy)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 3 h / 80 °C

1.2: 6 h / 170 - 180 °C

2.1: thionyl chloride / methanol / 2 h / 0 - 60 °C

With thionyl chloride; sodium methylate; In methanol;