2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

Base Information

Chemical Name:2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate
CAS No.:300767-55-9
Molecular Formula:C₁₈H₂₈O₄Si
Molecular Weight:336.503
Hs Code.:

Synonyms:2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

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Chemical Property of 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

Chemical Property:

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Technology Process of 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

There total 3 articles about 2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 108-24-7
acetic anhydride

: 300767-54-8
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenol

: 300767-55-9
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

Guidance literature:: With dmap; TEA; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1248/cpb.48.1138

Reference yield:

: 531-59-9
7-methoxycoumarin

: 300767-55-9
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 39 percent / LAH / diethyl ether / 0.25 h / 0 °C

2: 80 percent / DMAP / tetrahydrofuran / 8 h / 0 °C

3: 99 percent / DMAP; TEA / CH₂Cl₂ / 1 h / 20 °C

With dmap; lithium aluminium tetrahydride; TEA; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1248/cpb.48.1138

Reference yield:

: 300767-53-7
2-[(Z)-3-hydroxy-1-propenyl]-5-methoxyphenol

: 300767-55-9
2-[(Z)-3-{[1-(tert-butyl)-1,1-dimethyl-silanyl]oxy}-1-propenyl]-5-methoxyphenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DMAP / tetrahydrofuran / 8 h / 0 °C

2: 99 percent / DMAP; TEA / CH₂Cl₂ / 1 h / 20 °C

With dmap; TEA; In tetrahydrofuran; dichloromethane;
DOI:10.1248/cpb.48.1138