C₅₄H₇₀O₁₁Si

Base Information

Chemical Name:C₅₄H₇₀O₁₁Si
CAS No.:1264756-68-4
Molecular Formula:C₅₄H₇₀O₁₁Si
Molecular Weight:923.229
Hs Code.:

C<sub>54</sub>H<sub>70</sub>O<sub>11</sub>Si

Synonyms:C₅₄H₇₀O₁₁Si

Suppliers and Price of C₅₄H₇₀O₁₁Si

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₄H₇₀O₁₁Si

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of C₅₄H₇₀O₁₁Si

There total 23 articles about C₅₄H₇₀O₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1331832-27-9
C₅₄H₇₂O₁₁Si

: 1264756-68-4
C₅₄H₇₀O₁₁Si

Guidance literature:: With Dess-Martin periodane; In dichloromethane; tert-butyl alcohol; at 20 ℃; for 1.75h;
DOI:10.1016/j.tet.2011.05.082

Reference yield: 91.0%

: 1264756-67-3
C₅₄H₇₂O₁₁Si

: 1264756-68-4
C₅₄H₇₀O₁₁Si

Guidance literature:: With Dess-Martin periodane; In dichloromethane; tert-butyl alcohol; at 20 ℃;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: C₄₄H₅₂O₅Si

: 1264756-68-4
C₅₄H₇₀O₁₁Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: water; potassium hydroxide / tetrahydrofuran; methanol

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

2.2: 20 °C

3.1: diisobutylaluminium hydride / dichloromethane / -78 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

5.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

8.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

9.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

9.2: 20 °C

10.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

11.1: diethyl ether / -78 °C

12.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 20 °C / Molecular sieve

13.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0 °C

13.2: -78 °C

14.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; tetrapropylammonium perruthennate; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; di-n-butylboryl trifluoromethanesulfonate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Swern oxidation / 2.2: Wittig reaction / 4.1: Sharpless asymmetric epoxidation / 6.1: Wittig reaction / 11.1: Grignard reaction / 14.1: Dess-Martin oxidation;
DOI:10.1016/j.tetlet.2010.11.127