N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

Base Information

Chemical Name:N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide
CAS No.:1311383-16-0
Molecular Formula:C₃₀H₃₇N₃O₃S
Molecular Weight:519.708
Hs Code.:

Synonyms:N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

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Chemical Property of N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

Chemical Property:

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Technology Process of N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

There total 5 articles about N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1311383-71-7
N-(4-butylphenyl)-4-methyl-3-(piperazine-1-carbonyl)benzenesulfonamide

: 529-20-4
2-methylphenyl aldehyde

: 1311383-16-0
N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

Guidance literature:: N-(4-butylphenyl)-4-methyl-3-(piperazine-1-carbonyl)benzenesulfonamide; 2-methylphenyl aldehyde; With acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; for 8h;

Reference yield:

: 89001-57-0
5-(chlorosulfonyl)-2-methylbenzenecarboxylic acid

: 1311383-16-0
N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: hydrogenchloride / methanol / 2 h / 20 °C

4.1: acetic acid / 1,2-dichloro-ethane / 0.5 h / 20 °C

4.2: 8 h / 20 °C

With pyridine; hydrogenchloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 104-13-2
4-Butylaniline

: 1311383-16-0
N-(4-butylphenyl)-4-methyl-3-(4-(2-methylbenzyl)piperazine-1-carbonyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: hydrogenchloride / methanol / 2 h / 20 °C

4.1: acetic acid / 1,2-dichloro-ethane / 0.5 h / 20 °C

4.2: 8 h / 20 °C

With pyridine; hydrogenchloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;