N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

Base Information

Chemical Name:N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine
CAS No.:610768-46-2
Molecular Formula:C₁₈H₂₄N₄O₄S₂
Molecular Weight:424.545
Hs Code.:

Synonyms:N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

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Technology Process of N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

There total 5 articles about N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 610768-33-7
(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)prop-2-en-1-ol

: 610768-46-2
N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ol0352862

Reference yield: 53.0%

: 220378-49-4
C₈H₁₃N₃O₃S

: 50487-71-3
4-methyl-N-(2-propenyl)benzenesulfonamide

: 610768-46-2
N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: 223571-74-2
methyl (E)-3-(1-(N,N-dimethylsulfamoyl)-1H-imidazol-4-yl)acrylate

: 610768-46-2
N-allyl-N-[(2E)-3-(1-dimethylsulfamoyl-1H-imidazol-4-yl)-prop-2-enyl]-N-tosylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / DIBAL-H / CH₂Cl₂; hexane / -78 - 20 °C

2: 53 percent / PPh₃; DEAD / tetrahydrofuran / 2 h / 20 °C

With diisobutylaluminium hydride; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ol0352862