(1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Base Information

• Chemical Name: (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan
• CAS No.: 76670-70-7
• Molecular Formula: C₁₃H₁₃NO₄S
• Molecular Weight: 279.317

Synonyms:(1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Chemical Property of (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

There total 13 articles about (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

DL-(1α,2α,4α,5α,6β,7α)-6-<(4-Methylphenylsulfonyl)amino>-3,8-dioxatricyclo<5.1.0.02,4>octan-5-ol-methansulfonat (112319-74-1) → (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.02,4.05,7>nonan (76670-70-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 2h; Heating;

Reference yield: 72.0%

(1α,2α,3β,4β,5α,6α)-2,5-Dibrom-7-(4-methylphenylsulfonyl)-7-azabicyclo<4.1.0>heptan-3,4-diol (112297-32-2) → (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.02,4.05,7>nonan (76670-70-7)

Guidance literature:

With sodium glycolate; In tetrahydrofuran; for 8h; Ambient temperature;

Reference yield: 70.0%

(1S,2S,4S,5S,6R,7R)-5-Bromo-8-(toluene-4-sulfonyl)-3-oxa-8-aza-tricyclo[5.1.0.02,4]octan-6-ol (76670-68-3,112346-56-2) → (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.02,4.05,7>nonan (76670-70-7)

Guidance literature:

With 2,6-dichloro-benzonitrile; In tetrahydrofuran; other bases : K-t-butylate, sodium glycolate;

DOI:10.1016/S0040-4039(00)78718-1

upstream raw materials:

(1S,2S,4S,5S,6R,7R)-5-Bromo-8-(toluene-4-sulfonyl)-3-oxa-8-aza-tricyclo[5.1.0.0^2,4]octan-6-ol

(1α,2α,4α,5α,7α,8α)-6,9-Bis(4-methylphenylsulfonyl)-3-oxa-6,9-diazatetracyclo<6.1.0.0^2,40^5,7>nonan

DL-(1α,2α,4α,5β,6α,7α)-6-Brom-3-(4-methylphenylsulfonyl)-8-oxa-3-azatricyclo<5.1.0.0^2,4>octan-5-ol

(1α,2α,3β,4β,5α,6α)-2,5-Dibrom-7-(4-methylphenylsulfonyl)-7-azabicyclo<4.1.0>heptan-3,4-diol

Downstream raw materials:

cis-trisoxirane

(Z,Z,Z)-7-(4-Methylphenylsulfonyl)-7H-1,4,7-dioxazonin

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 76670-70-7 (1α,2α,4α,5α,7α,8α)-9-(4-Methylphenylsulfonyl)-3,6-dioxa-9-azatetracyclo<6.1.0.0^2,4.0^5,7>nonan

Send

Send

Metric Ton KG G Pound L ML

Send

Send