N(C₂H₅)4⁽¹⁺⁾*W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)^(1-) = (N(C₂H₅)4)(W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3))

Base Information

• Chemical Name: N(C₂H₅)4⁽¹⁺⁾*W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)^(1-) = (N(C₂H₅)4)(W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3))
• CAS No.: 205305-57-3
• Molecular Formula: C₈H₂₀N*C₂₈H₂₇OS₄SiW
• Molecular Weight: 849.975

Synonyms:N(C₂H₅)4⁽¹⁺⁾*W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)^(1-) = (N(C₂H₅)4)(W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3))

Chemical Property of N(C₂H₅)4⁽¹⁺⁾*W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)^(1-) = (N(C₂H₅)4)(W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3))

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Technology Process of N(C₂H₅)4⁽¹⁺⁾*W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)^(1-) = (N(C₂H₅)4)(W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3))

There total 3 articles about N(C₂H₅)4⁽¹⁺⁾*W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)^(1-) = (N(C₂H₅)4)(W(C₆H₄S₂)2(OSi(C₆H₅)2C(CH₃)3)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

2N(C2H5)4(1+)*{WO(S2C6H4)2}(2-)=(N(C2H5)4)2{WO(S2C6H4)2} + tert-butylchlorodiphenylsilane (58479-61-1) → N(C2H5)4(1+)*W(C6H4S2)2(OSi(C6H5)2C(CH3)3)(1-) = (N(C2H5)4)(W(C6H4S2)2(OSi(C6H5)2C(CH3)3)) (205305-57-3)

Guidance literature:

In acetonitrile; 1 h;

DOI:10.1021/ja973917f

Reference yield:

hexamethyldisilathiane (3385-94-2) + N(C2H5)4(1+)*WO(OSi(C6H5)2C(CH3)3)(C6H4S2)2(1-) = (N(C2H5)4)(WO(OSi(C6H5)2C(CH3)3)(C6H4S2)2) → N(C2H5)4(1+)*W(C6H4S2)2(OSi(C6H5)2C(CH3)3)(1-) = (N(C2H5)4)(W(C6H4S2)2(OSi(C6H5)2C(CH3)3)) (205305-57-3) + N(C2H5)4(1+)*WS(OSi(C6H5)2(C(CH3)3))(C6H4S2)2(1-) = (N(C2H5)4)[WS(OSi(C6H5)2(C(CH3)3))(C6H4S2)2]

Guidance literature:

In acetonitrile; (N2); addn. of S(SiMe3)2 to a soln. of W complex in CH3CN, stirring (2 d); solvent removal 8vac.), trituration (ether), drying (vac.); mixture (single crystals for X-ray diffraction could be obtained from DMF/ether);

DOI:10.1021/ja981015o

Reference yield:

N(C2H5)4(1+)*WO(OSi(C6H5)2C(CH3)3)(C6H4S2)2(1-) = (N(C2H5)4)(WO(OSi(C6H5)2C(CH3)3)(C6H4S2)2) + dibenzyltrisulfide (6493-73-8) → N(C2H5)4(1+)*W(C6H4S2)2(OSi(C6H5)2C(CH3)3)(1-) = (N(C2H5)4)(W(C6H4S2)2(OSi(C6H5)2C(CH3)3)) (205305-57-3) + N(C2H5)4(1+)*WS(OSi(C6H5)2(C(CH3)3))(C6H4S2)2(1-) = (N(C2H5)4)[WS(OSi(C6H5)2(C(CH3)3))(C6H4S2)2]

Guidance literature:

In acetonitrile; (N2); addn. of W complex to S(SCH2Ph)2 in CH3CN, stirring (6 h); solvent removal 8vac.), trituration (ether), drying (vac.); mixture (single crystals for X-ray diffraction could be obtained from DMF/ether);

DOI:10.1021/ja981015o

upstream raw materials:

hexamethyldisilathiane

dibenzyltrisulfide

tert-butylchlorodiphenylsilane

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