(S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

Base Information

Chemical Name:(S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane
CAS No.:185429-86-1
Molecular Formula:C₁₉H₂₄O₇S₂
Molecular Weight:432.496
Hs Code.:

(S)-1-(2H<sub>2</sub>)-4-(2H<sub>2</sub>)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

Synonyms:(S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

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Technology Process of (S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

There total 3 articles about (S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 98-59-9
p-toluenesulfonyl chloride

: 185429-84-9
(S)-1-(2H₂)-4-(2H₂)-2-methyl-1,2,4-trihydroxybutane

: 185429-86-1
(S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

Guidance literature:: With pyridine; for 18h;
DOI:10.1016/S0960-894X(96)00489-1

Reference yield:

: 6236-10-8,2306-22-1
(R)-(-)-citramalic acid

: 185429-86-1
(S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

Guidance literature:: Multi-step reaction with 3 steps

1: methanol

2: lithium aluminium deuteride / tetrahydrofuran

3: 4 Angstroem molecular sieves, pyridine

With pyridine; lithium aluminium deuteride; 4 A molecular sieve; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(97)00690-X

Reference yield:

: 81426-68-8
(R)-dimethyl 2-hydroxy-2-methylsuccinate

: 185429-86-1
(S)-1-(2H₂)-4-(2H₂)-bis-1,4-(p-toluenesulfonyloxy)-2-hydroxy-2-methylbutane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium deuteride / tetrahydrofuran

2: 4 Angstroem molecular sieves, pyridine

With pyridine; lithium aluminium deuteride; 4 A molecular sieve; In tetrahydrofuran;
DOI:10.1016/S0040-4020(97)00690-X