N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid

Base Information

• Chemical Name: N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid
• CAS No.: 1586819-27-3
• Molecular Formula: C₂₆H₁₄Cl₆N₂O₄
• Molecular Weight: 631.126

Synonyms:N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid

Chemical Property of N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid

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Technology Process of N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid

There total 4 articles about N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

maleic anhydride (108-31-6) + N-[4-(4-aminobenzyl)phenyl]imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid (1430747-66-2) → N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid (1586819-27-3)

Guidance literature:

In N,N-dimethyl-formamide; at 150 ℃; for 6h;

DOI:10.1134/S1070428014020122

Reference yield:

4,4'-diamino diphenyl methane (101-77-9) → N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid (1586819-27-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 6 h / 150 °C

2: N,N-dimethyl-formamide / 6 h / 150 °C

In N,N-dimethyl-formamide;

DOI:10.1134/S1070428014020122

Reference yield:

1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride (1217537-92-2) → N-{4-[4-(maleimido)benzyl]phenyl}imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid (1586819-27-3)

Guidance literature:

Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 6 h / 150 °C

2: N,N-dimethyl-formamide / 6 h / 150 °C

In N,N-dimethyl-formamide;

DOI:10.1134/S1070428014020122

upstream raw materials:

1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid anhydride

4,4'-diamino diphenyl methane

maleic anhydride

N-[4-(4-aminobenzyl)phenyl]imide of 1,4,5,6,7,7-hexachlorobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid

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