β-azido-meso-tetraphenylporphyrinatonickel(II)

Base Information

Chemical Name:β-azido-meso-tetraphenylporphyrinatonickel(II)
CAS No.:936548-03-7
Molecular Formula:C₄₄H₂₇N₇Ni
Molecular Weight:712.435
Hs Code.:

Synonyms:β-azido-meso-tetraphenylporphyrinatonickel(II)

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Chemical Property of β-azido-meso-tetraphenylporphyrinatonickel(II)

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Technology Process of β-azido-meso-tetraphenylporphyrinatonickel(II)

There total 1 articles about β-azido-meso-tetraphenylporphyrinatonickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: C₄₄H₃₀N₆

: 936548-03-7
β-azido-meso-tetraphenylporphyrinatonickel(II)

Guidance literature:: C₄₄H₃₀N₆; With sulfuric acid; sodium nitrite; In tetrahydrofuran; water; at 20 ℃; for 0.5h; Inert atmosphere;

With sodium azide; In water; at 20 ℃; for 0.5h;
DOI:10.1039/b901309a

Reference yield: 82.0%

: 2396-65-8
1,8-nonadiyn

: 936548-03-7
β-azido-meso-tetraphenylporphyrinatonickel(II)

: nickel(II)-2-[4-(hept-6-ynyl)-1,2,3-triazol-4-yl]-5,10,15,20-tetraphenylporphyrin

Guidance literature:: With copper(II) sulfate; ascorbic acid; In water; N,N-dimethyl-formamide; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1039/b901309a

Reference yield: 82.0%

: 2396-65-8
1,8-nonadiyn

: 936548-03-7
β-azido-meso-tetraphenylporphyrinatonickel(II)

: 1168135-88-3
2-[4-(hept-6-ynyl)-1,2,3-triazolo]-5,10,15,20-tetraphenylporphyrinatonickel(II)

Guidance literature:: With copper(II) sulfate; ascorbic acid; In N,N-dimethyl-formamide; under Ar; 1,8-nonadiyne added to soln. of Ni complex, Cu salt and ascorbic acid in DMF, mixt. stirred at 50°C for 24 h; CH2Cl2 added, org. phase sepd. and washed with aq. K2CO3 and H2O, dried over Na2SO4, filtrate evapd. under vac., chromy. (silica gel, CH2Cl2/petroleum ether);
DOI:10.1039/b901309a