complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone

Base Information

• Chemical Name: complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone
• CAS No.: 110638-47-6
• Molecular Formula: C₈Cl₂N₂O₂*C₁₆H₁₂S₄
• Molecular Weight: 559.541

Synonyms:complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone

Chemical Property of complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone

Chemical Property:

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Technology Process of complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone

There total 1 articles about complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,6-dithiapyrene (194-07-0) → complex of 2,7-bis(methylthio)-1,6-dithiapyrene and 2,3-dichloro-5,6-dicyano-p-benzoquinone (110638-47-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / n-BuLi / tetrahydrofuran; hexane / 1.) 45 min, -70 deg C, 2.) 1.5 h, from -70 deg C to room temperature

2: CH₂Cl₂

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;

DOI:10.1021/ja00257a011

upstream raw materials:

1,6-dithiapyrene

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