Technology Process of C35H57N3O11Si2
There total 7 articles about C35H57N3O11Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 25 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/jo202061t
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / water; acetonitrile / 0.67 h / 25 °C / Inert atmosphere
2.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere
3.1: methanol / dichloromethane / 4 h / 0 °C / Inert atmosphere
3.2: 0.08 h / 20 °C / Inert atmosphere
4.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 25 °C / Inert atmosphere
With
methanol; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; palladium 10% on activated carbon; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo202061t
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: methanol / dichloromethane / 4 h / 0 °C / Inert atmosphere
1.2: 0.08 h / 20 °C / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / methanol / 0.5 h / 25 °C / Inert atmosphere
With
methanol; palladium 10% on activated carbon; hydrogen;
In
methanol; dichloromethane;
DOI:10.1021/jo202061t
