C₆₆H₁₀₆N₆O₁₆Si

Base Information

Chemical Name:C₆₆H₁₀₆N₆O₁₆Si
CAS No.:327159-94-4
Molecular Formula:C₆₆H₁₀₆N₆O₁₆Si
Molecular Weight:1267.68
Hs Code.:

C<sub>66</sub>H<sub>106</sub>N<sub>6</sub>O<sub>16</sub>Si

Synonyms:C₆₆H₁₀₆N₆O₁₆Si

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Chemical Property of C₆₆H₁₀₆N₆O₁₆Si

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Technology Process of C₆₆H₁₀₆N₆O₁₆Si

There total 4 articles about C₆₆H₁₀₆N₆O₁₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 327159-93-3
C₆₆H₁₀₈N₆O₁₇Si

: 327159-94-4
C₆₆H₁₀₆N₆O₁₆Si

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In dichloromethane;
DOI:10.1016/S0960-894X(00)00585-0

Reference yield:

: C₆₉H₁₀₉Cl₃N₆O₁₈Si

: 327159-94-4
C₆₆H₁₀₆N₆O₁₆Si

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / KMnO₄; NaH₂PO₄ / 2-methyl-propan-2-ol

2: 100 percent / Zn; aq. AcOH

3: 55 percent / HATU; DIEA / CH₂Cl₂

With potassium permanganate; sodium dihydrogenphosphate; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; zinc; In dichloromethane; tert-butyl alcohol;
DOI:10.1016/S0960-894X(00)00585-0

Reference yield:

: 327159-92-2
C₆₉H₁₀₉Cl₃N₆O₁₉Si

: 327159-94-4
C₆₆H₁₀₆N₆O₁₆Si

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Zn; aq. AcOH

2: 55 percent / HATU; DIEA / CH₂Cl₂

With acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; zinc; In dichloromethane;
DOI:10.1016/S0960-894X(00)00585-0