3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

Base Information

Chemical Name:3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one
CAS No.:1025906-30-2
Molecular Formula:C₃₅H₃₆O₇
Molecular Weight:568.667
Hs Code.:

Synonyms:3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

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Chemical Property of 3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

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Technology Process of 3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

There total 4 articles about 3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92831-74-8
4-<<4-(benzyloxy)-3-methoxyphenyl>methyl>dihydro-2(3H)-furanone

: 651340-08-8
3-(benzyloxy)-4,5-dimethoxybenzyl bromide

: 1025906-30-2
3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -35 ℃; for 0.75h;
DOI:10.1039/b304411d

Reference yield:

: 7632-62-4
3-benzyloxy-4,5-dimethoxybenzyl alcohol

: 1025906-30-2
3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / diethyl ether / 1 h / 20 °C

2: lithium hexamethyldisilazanide / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.75 h / -35 °C

With phosphorus tribromide; lithium hexamethyldisilazane; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether;
DOI:10.1039/b304411d

Reference yield:

: 29865-90-5
3-hydroxy-4,5-dimethoxybenzaldehyde

: 1025906-30-2
3-(3-benzyloxy-4,5-dimethoxy-benzyl)-4-(4-benzyloxy-3-methoxy-benzyl)-dihydro-furan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide / 4 h / 70 °C

2: NaBH₄ / methanol / 0.17 h / 20 °C

3: PBr₃ / diethyl ether / 1 h / 20 °C

4: lithium hexamethyldisilazanide / tetrahydrofuran; hexamethylphosphoric acid triamide / 0.75 h / -35 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1039/b304411d