N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Base Information

• Chemical Name: N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide
• CAS No.: 1579268-76-0
• Molecular Formula: C₃₃H₃₃ClN₂O₆S₂
• Molecular Weight: 653.22

Synonyms:N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Chemical Property of N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide

There total 1 articles about N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

5-chloro-1-p-toluenesulfonylindole (32617-55-3) + C18H21NO4S (1378478-43-3) → N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide (1579268-76-0)

Guidance literature:

5-chloro-1-p-toluenesulfonylindole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

C₁₈H₂₁NO₄S; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

DOI:10.1016/j.tet.2014.01.074

Reference yield: 88.0%

N-(3-(5-chloro-1-tosyl-1H-indol-2-yl)-3-hydroxypropyl)-N-(4-methoxybenzyl)-4-methylbenzenesulfonamide (1579268-76-0) → 9-chloro-5-(4-methoxyphenyl)-2,6-ditosyl-1,2,3,4,5,6-hexahydroazepino[4,3-b]indole (1579269-00-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 11h;

DOI:10.1016/j.tet.2014.01.074

upstream raw materials:

5-chloro-1-p-toluenesulfonylindole

C₁₈H₂₁NO₄S

Downstream raw materials:

9-chloro-5-(4-methoxyphenyl)-2,6-ditosyl-1,2,3,4,5,6-hexahydroazepino[4,3-b]indole

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