bis(3-hydroxyphenyl)arsinous bromide

Base Information

• Chemical Name: bis(3-hydroxyphenyl)arsinous bromide
• CAS No.: 6308-60-7
• Molecular Formula: C₁₂H₁₀AsBrO₂
• Molecular Weight: 341.036
• Mol file: 6308-60-7.mol

Synonyms:

Chemical Property of bis(3-hydroxyphenyl)arsinous bromide

Chemical Property:

• Vapor Pressure: 2.09E-09mmHg at 25°C
• Boiling Point: 468.7°Cat760mmHg
• Flash Point: 237.3°C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of bis(3-hydroxyphenyl)arsinous bromide

There total 2 articles about bis(3-hydroxyphenyl)arsinous bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis-(3-hydroxy-phenyl)-arsinic acid (6308-62-9) → bromo-bis-(3-hydroxy-phenyl)-arsine (6308-60-7)

Guidance literature:

With water; hydrogen bromide; hydrogen iodide; acetic acid; Reagens 4: Schwefeldioxid;

DOI:10.1021/ja01318a044

Reference yield:

bis-(3-amino-phenyl)-arsinic acid (856623-73-9) → bromo-bis-(3-hydroxy-phenyl)-arsine (6308-60-7)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous sulfuric acid; sodium nitrite / anscliessend Erwaermen

2: water; acetic acid; aqueous hydriodic acid; hydrobromic acid / Reagens 4: Schwefeldioxid

With sulfuric acid; water; hydrogen bromide; hydrogen iodide; acetic acid; sodium nitrite;

DOI:10.1021/ja01318a044

upstream raw materials:

bis-(3-hydroxy-phenyl)-arsinic acid

bis-(3-amino-phenyl)-arsinic acid