1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne

Base Information

• Chemical Name: 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne
• CAS No.: 1238279-11-2
• Molecular Formula: C₂₅H₂₇N₃O₄S₂
• Molecular Weight: 497.639
• Mol file: 1238279-11-2.mol

Synonyms:1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne

Chemical Property of 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne

There total 1 articles about 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N,N'-bis[(4-methylphenyl)sulfonyl]-N'-(2-cyanoethyl)-2-butyne-1,4-diamine (1238279-18-9) + 1-Bromo-2-butyne (3355-28-0) → 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne (1238279-11-2)

Guidance literature:

With potassium carbonate; In acetonitrile; for 6h; Reflux;

DOI:10.1002/ejoc.200901318

Reference yield: 81.0%

1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazadeca-3,8-diyne (1238279-11-2) → C25H27N3O4S2 (1238279-25-8)

Guidance literature:

With Wilkinson's catalyst; In toluene; at 90 ℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Sealed vial;

DOI:10.1002/ejoc.200901318

upstream raw materials:

N,N'-bis[(4-methylphenyl)sulfonyl]-N'-(2-cyanoethyl)-2-butyne-1,4-diamine

1-Bromo-2-butyne

Downstream raw materials:

C₂₅H₂₇N₃O₄S₂